8W7Y
Crystal structure of GcCGT in complex with UDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-05-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 63.743, 63.743, 231.812 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 55.200 - 2.400 |
R-factor | 0.1931 |
Rwork | 0.191 |
R-free | 0.24440 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.606 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.950 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.143 | 1.435 |
Rmeas | 0.150 | 1.508 |
Rpim | 0.047 | 0.458 |
Total number of observations | 212061 | 24224 |
Number of reflections | 21244 | 2276 |
<I/σ(I)> | 13.3 | 1.9 |
Completeness [%] | 94.8 | |
Redundancy | 10 | 10.6 |
CC(1/2) | 0.998 | 0.707 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2.2 M Sodium malonate, pH 7.6 |