8VY8
Recombinant alpha bungarotoxin complexed with HAP peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-05-08 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.541 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.529, 73.110, 79.840 |
Unit cell angles | 90.00, 103.68, 90.00 |
Refinement procedure
Resolution | 53.200 - 2.400 |
R-factor | 0.239 |
Rwork | 0.237 |
R-free | 0.27730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.166 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.200 | 2.486 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.148 | 0.416 |
Number of reflections | 18053 | 1768 |
<I/σ(I)> | 10.58 | |
Completeness [%] | 96.3 | |
Redundancy | 7.6 | |
CC(1/2) | 0.992 | 0.943 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 0.1 M HEPES (pH 7.5), 35% PEG3350, 0.2 M MgCl2. 18 degree centigrade |