8VSX

NMR Structure of GCAP5 R22A

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600
2	Bruker	AVANCE III		800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	3	2D 1H-15N HSQC
10	1	2	2D (HB)CB(CGCD)HD
11	1	2	3D C(CO)NH
12	1	2	3D HCCH-TOCSY
13	1	2	2D 1H-13C HSQC aliphatic
14	1	2	2D HBCBCGCDCEHE
15	1	2	3D 1H-13C NOESY aliphatic
2	1	2	3D HNCO
3	1	2	3D HNCACB
4	1	2	3D HNCA
5	1	2	3D CBCA(CO)NH
6	1	2	3D HBHANH
7	1	2	3D HBHA(CO)NH
8	1	2	3D HN(COCA)CB
9	1	2	3D HNCACBi

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7.4	1	305

Conformers

Conformers Calculated Total Number	500
Conformers Submitted Total Number	10