8VPX
UIC-10-BPE extension of UIC-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-24 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.688839 |
Spacegroup name | P 1 |
Unit cell lengths | 10.305, 17.610, 26.616 |
Unit cell angles | 99.46, 99.72, 95.85 |
Refinement procedure
Resolution | 17.220 - 1.451 |
R-factor | 0.1299 |
Rwork | 0.123 |
R-free | 0.18140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.641 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.220 | 1.502 |
High resolution limit [Å] | 1.451 | 1.451 |
Number of reflections | 2572 | 173 |
<I/σ(I)> | 28.56 | |
Completeness [%] | 80.2 | |
Redundancy | 3.7 | |
CC(1/2) | 0.999 | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SLOW COOLING | 298 | Methanol, acetonitrile, water |