8VPE

UIC-10-BIF extension of UIC-1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-D
Synchrotron site	APS
Beamline	21-ID-D
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-10-28
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.6199
Spacegroup name	P 21 21 21
Unit cell lengths	10.764, 36.020, 47.455
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	16.840 - 0.910
R-factor	0.0965
Rwork	0.095
R-free	0.11140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.938
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	16.840	0.943
High resolution limit [Å]	0.910	0.910
Number of reflections	13878	1314
<I/σ(I)>	21.69
Completeness [%]	99.2
Redundancy	12.8
CC(1/2)	0.998	0.979

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	Acetonitrile, water