8VD3
Crystal Structure of D14 from Arabidopsis thaliana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 298 |
Detector technology | PIXEL |
Collection date | 2019-12-12 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 1.00 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.692, 69.267, 90.800 |
Unit cell angles | 90.00, 93.38, 90.00 |
Refinement procedure
Resolution | 45.320 - 2.000 |
R-factor | 0.16495 |
Rwork | 0.163 |
R-free | 0.20724 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.559 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.320 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 36532 | 2459 |
<I/σ(I)> | 14.6 | |
Completeness [%] | 99.3 | |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.15M Ammonium acetate, 0.01M Calcium chloride dihydrate, 0.1M Tris pH 8.5, 28% broad PEG smear from BCS (Molecular Dimensions) |