8V96
GII.14 M7 norovirus protruding domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2023-06-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95373 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 105.818, 91.835, 67.106 |
Unit cell angles | 90.00, 92.98, 90.00 |
Refinement procedure
Resolution | 42.580 - 1.440 |
R-factor | 0.2081 |
Rwork | 0.207 |
R-free | 0.23140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.061 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.020 | 1.460 |
High resolution limit [Å] | 1.440 | 1.440 |
Rmerge | 0.119 | 1.939 |
Rmeas | 0.141 | 2.302 |
Rpim | 0.076 | 1.228 |
Total number of observations | 381270 | 17145 |
Number of reflections | 113736 | 5241 |
<I/σ(I)> | 6.5 | 0.6 |
Completeness [%] | 98.4 | |
Redundancy | 3.4 | 3.3 |
CC(1/2) | 0.993 | 0.163 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 0.1 M BICINE 10% v/v MPD |