8V95
GII.8 Amsterdam norovirus protruding domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2023-06-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95373 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.230, 78.428, 115.387 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.680 - 1.730 |
R-factor | 0.1757 |
Rwork | 0.174 |
R-free | 0.20370 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.881 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.680 | 1.760 |
High resolution limit [Å] | 1.730 | 1.730 |
Rmerge | 0.089 | 0.647 |
Rmeas | 0.098 | 0.713 |
Rpim | 0.040 | 0.294 |
Total number of observations | 375331 | 16109 |
Number of reflections | 64062 | 3023 |
<I/σ(I)> | 8.8 | 1.4 |
Completeness [%] | 99.2 | |
Redundancy | 5.9 | 5.3 |
CC(1/2) | 0.998 | 0.810 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 0.2 M Sodium chloride 0.1 M Sodium/potassium phosphate (pH 6.2) 50% v/v PEG 200 |