8V7K
Human DNA polymerase eta-DNA-araC-ended primer ternary complex:reaction with 10 mM Mn2+ for 1800s
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-17 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.1272 |
Spacegroup name | P 61 |
Unit cell lengths | 98.520, 98.520, 81.652 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.810 - 1.650 |
R-factor | 0.2069 |
Rwork | 0.206 |
R-free | 0.23280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.321 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.810 | 37.810 | 1.750 |
High resolution limit [Å] | 1.650 | 4.940 | 1.650 |
Rmerge | 0.065 | 0.035 | 0.869 |
Rmeas | 0.068 | 0.037 | 0.916 |
Number of reflections | 53654 | 3958 | 17039 |
<I/σ(I)> | 19.33 | ||
Completeness [%] | 99.9 | ||
Redundancy | 20.3 | ||
CC(1/2) | 0.999 | 0.999 | 0.814 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | PEG 2000MME, 0.1 M MES |