8V7F
Human DNA polymerase eta-DNA-araC-ended primer-dAMPNPP ternary complex with Mn2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2022-09-21 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 0.9786 |
Spacegroup name | P 61 |
Unit cell lengths | 98.700, 98.700, 82.324 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.740 - 2.200 |
R-factor | 0.2049 |
Rwork | 0.203 |
R-free | 0.25170 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.788 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.740 | 42.740 | 2.330 |
High resolution limit [Å] | 2.200 | 6.530 | 2.200 |
Rmerge | 0.086 | 0.029 | 0.660 |
Rmeas | 0.095 | 0.032 | 0.724 |
Number of reflections | 23247 | 1710 | 7254 |
<I/σ(I)> | 15.9 | ||
Completeness [%] | 99.0 | ||
Redundancy | 11.4 | ||
CC(1/2) | 0.998 | 0.990 | 0.804 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | PEG 2000MME, 0.1 M MES |