8V3E
Structure of Myroides odoratus phage Tad2 in apo state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2023-04-13 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | H 3 2 |
Unit cell lengths | 93.206, 93.206, 235.549 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.570 - 2.390 |
R-factor | 0.2316 |
Rwork | 0.227 |
R-free | 0.27330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.432 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | AutoSol |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.570 | 2.480 |
High resolution limit [Å] | 2.390 | 2.390 |
Rpim | 0.039 | 0.071 |
Number of reflections | 109160 | 15778 |
<I/σ(I)> | 11.9 | |
Completeness [%] | 99.0 | |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | magnesium chloride, sodium acetate, PEG 400 |