8UIW
yjdF riboswitch from R. gauvreauii in complex with chelerythrine bound to Fab BL3-6 S97N
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-08 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 1.000300 |
Spacegroup name | P 1 |
Unit cell lengths | 65.792, 77.438, 95.848 |
Unit cell angles | 87.19, 88.43, 88.05 |
Refinement procedure
Resolution | 95.700 - 2.770 |
R-factor | 0.212 |
Rwork | 0.211 |
R-free | 0.23100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.357 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.700 | 2.860 |
High resolution limit [Å] | 2.770 | 2.770 |
Rmerge | 0.052 | 1.748 |
Rmeas | 0.057 | 1.935 |
Rpim | 0.025 | 0.823 |
Number of reflections | 87020 | 8106 |
<I/σ(I)> | 18.6 | |
Completeness [%] | 93.6 | 90.3 |
Redundancy | 5.6 | 5.3 |
CC(1/2) | 0.993 | 0.524 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 0.1 M HEPES pH 7.5, 0.2 M ammonium acetate, 25% PEG 3350 |