8UEL
Crystal structure of enolase from Litopenaeus vannamei
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL02U1 |
Synchrotron site | SSRF |
Beamline | BL02U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-01-17 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 1.276911 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.613, 86.571, 155.881 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.680 - 2.490 |
R-factor | 0.1712 |
Rwork | 0.168 |
R-free | 0.22440 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.925 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 10.000 | 2.540 |
High resolution limit [Å] | 2.490 | 6.760 | 2.500 |
Rmerge | 0.180 | 0.086 | 0.641 |
Rmeas | 0.196 | 0.094 | 0.702 |
Rpim | 0.077 | 0.039 | 0.285 |
Number of reflections | 38505 | 2105 | 1871 |
<I/σ(I)> | 4 | ||
Completeness [%] | 100.0 | 100 | 99.9 |
Redundancy | 6.4 | 5.8 | 5.9 |
CC(1/2) | 0.982 | 0.992 | 0.868 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | (NH4)2SO4, MES pH 6.5, PEG 5000 monomethyl ether |