8U5L
MAU868, a novel human-derived monoclonal neutralizing antibody targeting BK virus VP1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2015-11-15 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 224.224, 224.224, 143.937 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 79.280 - 2.700 |
R-factor | 0.1846 |
Rwork | 0.183 |
R-free | 0.21650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.568 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.280 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.275 | 1.382 |
Rmeas | 0.280 | 1.410 |
Rpim | 0.054 | 0.275 |
Total number of observations | 2655968 | 369148 |
Number of reflections | 100483 | 14325 |
<I/σ(I)> | 14.8 | 3.1 |
Completeness [%] | 99.8 | |
Redundancy | 26.4 | 25.8 |
CC(1/2) | 0.998 | 0.838 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291.1 | 0.2M MgCl 2 25% w/v Peg 3350 0.1M Bis-Tris pH 7.0 |