8TV2
Structure of apo FabS1C_L1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-11-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 74.259, 74.259, 370.837 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 64.310 - 2.650 |
R-factor | 0.207 |
Rwork | 0.204 |
R-free | 0.24730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.197 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 92.710 | 2.780 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.128 | 1.136 |
Rmeas | 0.136 | 1.209 |
Rpim | 0.045 | 0.405 |
Number of reflections | 33902 | 3816 |
<I/σ(I)> | 9.3 | 1.9 |
Completeness [%] | 94.1 | 82.3 |
Redundancy | 8.9 | 8.7 |
CC(1/2) | 0.994 | 0.702 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 18% PEG6000, 1M Lithium Chloride, 100 mM Sodium citrate 5.0 |