8T3J
Crystal structure of native exfoliative toxin C (ExhC) from Mammaliicoccus sciuri
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LNLS SIRIUS BEAMLINE MANACA |
Synchrotron site | LNLS SIRIUS |
Beamline | MANACA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-06-03 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.977180 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 167.094, 167.094, 157.743 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.283 - 2.705 |
Rwork | 0.211 |
R-free | 0.27010 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.546 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0411) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.283 | 2.807 |
High resolution limit [Å] | 2.705 | 2.710 |
Rpim | 0.067 | 0.752 |
Number of reflections | 30672 | 3017 |
<I/σ(I)> | 8.4 | 0.79 |
Completeness [%] | 99.9 | |
Redundancy | 26.2 | |
CC(1/2) | 0.995 | 0.450 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 0.1 M HEPES pH 7.5 and 0.8 M Potassium/Sodium tartrate |