8SZX
Crystal structure of b'-WD40 Lys17Ala mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS-II BEAMLINE 17-ID-1 |
Synchrotron site | NSLS-II |
Beamline | 17-ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-05-22 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.92 |
Spacegroup name | I 41 |
Unit cell lengths | 158.189, 158.189, 47.567 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.960 - 2.000 |
R-factor | 0.1921 |
Rwork | 0.190 |
R-free | 0.23350 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.644 |
Data reduction software | HKL-3000 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.960 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 40138 | 2931 |
<I/σ(I)> | 3.9 | 1.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 4.7 | 4.7 |
CC(1/2) | 0.955 | 0.683 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295.15 | 0.1M MES pH 6.5, PEG 19% 20000 |