8SWZ
PARP4 ART domain bound to EB47
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-05 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.12 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 116.848, 150.859, 104.613 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 69.240 - 3.000 |
R-factor | 0.2058 |
Rwork | 0.203 |
R-free | 0.24830 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.559 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.240 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.114 | 2.022 |
Rmeas | 0.118 | 2.096 |
Rpim | 0.031 | 0.547 |
Total number of observations | 43823 | |
Number of reflections | 35783 | 3020 |
<I/σ(I)> | 18.2 | 1.4 |
Completeness [%] | 100.0 | |
Redundancy | 14.5 | 14.5 |
CC(1/2) | 0.999 | 0.521 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG3350, 0.2M sodium citrate tribasic dihydrate, 800uM EB47 |