8SJM
[3T12] Self-assembling left-handed tensegrity triangle with 12 interjunction base pairs and R3 symmetry
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-12 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | H 3 |
Unit cell lengths | 162.319, 162.319, 109.158 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.860 - 8.080 |
R-factor | 0.1093 |
Rwork | 0.108 |
R-free | 0.14750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5w6w |
RMSD bond length | 0.004 |
RMSD bond angle | 0.678 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 86.216 | 86.216 | 9.621 |
High resolution limit [Å] | 8.080 | 14.039 | 8.080 |
Number of reflections | 858 | 216 | 216 |
<I/σ(I)> | 5.7 | 14.2 | 1.1 |
Completeness [%] | 82.7 | ||
Redundancy | 6.8 | 7.6 | |
CC(1/2) | 0.998 | 0.998 | 0.430 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293 | 100 mM MOPS, 1.25 M magnesium sulfate |