8SIU
Origin Recognition Complex Associated (ORCA) protein bound to Orc2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-02 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.979092 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 91.023, 135.431, 78.567 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.510 - 1.800 |
R-factor | 0.1712 |
Rwork | 0.170 |
R-free | 0.20320 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.091 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.510 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 45458 | 2577 |
<I/σ(I)> | 14.8 | 1.1 |
Completeness [%] | 99.8 | 97.4 |
Redundancy | 39 | |
CC(1/2) | 0.999 | 0.505 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 1.2 M ammonium sulfate, 100 mM MES pH 5.3 |