8S8Y
OPR3 variant R283E in its dimeric form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-08 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.8856 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.227, 90.357, 78.128 |
Unit cell angles | 90.00, 107.97, 90.00 |
Refinement procedure
Resolution | 44.800 - 1.800 |
Rwork | 0.187 |
R-free | 0.21960 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.21_5207: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.800 | 1.780 |
High resolution limit [Å] | 1.750 | 1.750 |
Rpim | 0.080 | 1.410 |
Number of reflections | 137014 | 2424 |
<I/σ(I)> | 5.72 | |
Completeness [%] | 97.6 | |
Redundancy | 3.5 | |
CC(1/2) | 0.994 | 0.150 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M MES/Tris (6.5), 50 mM ammonium sulfate, 8-16% PEG8000 |