8S8S

An induced-fit motion of a mobile loop

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-12-10
Detector	DECTRIS PILATUS 200K
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	44.272, 58.059, 82.383
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.458 - 1.314
R-factor	0.1889
Rwork	0.188
R-free	0.20950
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.760
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.460	47.460
High resolution limit [Å]	1.314	1.314
Number of reflections	49373	49373
<I/σ(I)>	12.86
Completeness [%]	96.2
Redundancy	12.3
CC(1/2)	0.999	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		277	ammonium phosphate