Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-X |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-02-20 |
| Detector | DECTRIS PILATUS 300K |
| Wavelength(s) | 1.54178 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 93.853, 93.853, 121.021 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.540 - 1.900 |
| R-factor | 0.18112 |
| Rwork | 0.179 |
| R-free | 0.22523 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.520 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 67.470 | 1.985 |
| High resolution limit [Å] | 1.896 | 1.896 |
| Rmeas | 0.180 | 1.600 |
| Number of reflections | 15176 | 691 |
| <I/σ(I)> | 11.9 | 1.4 |
| Completeness [%] | 96.3 | 72.7 |
| Redundancy | 9.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | 30% PEG 3350 0.1M pH=9 NaH2PO4/Na2HPO4 |
