8S3G
Atomic structure of truncated worm GdH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-01-24 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.87313 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 151.245, 151.245, 146.043 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 97.510 - 2.290 |
R-factor | 0.2252 |
Rwork | 0.224 |
R-free | 0.24780 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.866 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 97.510 | 2.320 |
High resolution limit [Å] | 2.290 | 2.290 |
Number of reflections | 167056 | 5279 |
<I/σ(I)> | 3.5 | |
Completeness [%] | 99.3 | |
Redundancy | 5.2 | |
CC(1/2) | 0.974 | 0.428 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.1M acetic acid ph 5.5 20% MPD |