8S3G
Atomic structure of truncated worm GdH
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-01-24 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.87313 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 151.245, 151.245, 146.043 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 97.510 - 2.290 |
| R-factor | 0.2252 |
| Rwork | 0.224 |
| R-free | 0.24780 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.866 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 97.510 | 2.320 |
| High resolution limit [Å] | 2.290 | 2.290 |
| Number of reflections | 167056 | 5279 |
| <I/σ(I)> | 3.5 | |
| Completeness [%] | 99.3 | |
| Redundancy | 5.2 | |
| CC(1/2) | 0.974 | 0.428 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.1M acetic acid ph 5.5 20% MPD |
