8S2X
SSX structure of Arabidopsis thaliana Pdx1.3 grown in microfluidic droplets
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2023-01-26 |
Detector | PSI JUNGFRAU 4M |
Wavelength(s) | 1.07 |
Spacegroup name | H 3 |
Unit cell lengths | 180.300, 180.300, 119.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 65.396 - 2.500 |
Rwork | 0.158 |
R-free | 0.18830 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.511 |
Data reduction software | CrystFEL (0.10.2) |
Data scaling software | CrystFEL (0.10.2) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 94.750 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 50011 | 4635 |
<I/σ(I)> | 5 | 0.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 44.2 | 44.2 |
CC(1/2) | 0.960 | 0.270 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROFLUIDIC | 7 | 294 | 600 mM Sodium citrate and 100 mM HEPES pH 7 |