Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-02-18 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97625 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.504, 213.257, 55.487 |
| Unit cell angles | 90.00, 95.99, 90.00 |
Refinement procedure
| Resolution | 45.300 - 2.190 |
| R-factor | 0.18042 |
| Rwork | 0.177 |
| R-free | 0.23838 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.495 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.300 | 2.260 |
| High resolution limit [Å] | 2.190 | 2.190 |
| Rmeas | 0.050 | 0.778 |
| Number of reflections | 52645 | 4168 |
| <I/σ(I)> | 13.1 | 1.6 |
| Completeness [%] | 98.0 | |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
