8S03

NMR solution structure of the CysD2 domain of MUC2

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III HD		900
2	Bruker	AVANCE III HD		800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-1H NOESY
10	1	3	2D 1H-13C HSQC15
2	1	2	2D 1H-15N HSQC
3	1	2	2D 1H-13C HSQC
4	1	2	3D HNCA
5	1	2	3D HN(CO)CA
6	1	2	3D HNCACB
7	1	2	3D HCCH-TOCSY
8	1	2	3D 1H-13C NOESY aliphatic
9	1	2	3D 1H-15N NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	Atmospheric pressure	318

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	10