Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-08-12 |
| Detector | DECTRIS EIGER2 XE 9M |
| Wavelength(s) | .92819 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 46.572, 216.554, 56.070 |
| Unit cell angles | 90.00, 96.69, 90.00 |
Refinement procedure
| Resolution | 108.280 - 2.170 |
| R-factor | 0.18289 |
| Rwork | 0.180 |
| R-free | 0.23148 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.287 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | CSearch |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 108.280 | 2.210 |
| High resolution limit [Å] | 2.170 | 2.170 |
| Rmeas | 0.074 | 1.090 |
| Number of reflections | 57530 | 3073 |
| <I/σ(I)> | 7.4 | |
| Completeness [%] | 99.8 | 99.8 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
