Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-07-20 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | .97242 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.813, 211.913, 55.539 |
| Unit cell angles | 90.00, 96.49, 90.00 |
Refinement procedure
| Resolution | 45.560 - 1.910 |
| R-factor | 0.17801 |
| Rwork | 0.176 |
| R-free | 0.22010 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.314 |
| Data reduction software | XDS (5.8.0232) |
| Data scaling software | Aimless |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.560 | 1.930 |
| High resolution limit [Å] | 1.910 | 1.910 |
| Rmeas | 0.047 | 0.933 |
| Number of reflections | 79049 | 1911 |
| <I/σ(I)> | 11.7 | 1.6 |
| Completeness [%] | 97.5 | 91.6 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
