Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-12-18 |
| Detector | DECTRIS EIGER2 S 16M |
| Wavelength(s) | 1.000040 |
| Spacegroup name | P 1 |
| Unit cell lengths | 53.479, 56.407, 67.792 |
| Unit cell angles | 72.88, 71.80, 84.32 |
Refinement procedure
| Resolution | 48.000 - 1.836 |
| R-factor | 0.2238 |
| Rwork | 0.223 |
| R-free | 0.24090 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.080 |
| Data reduction software | autoPROC (1.1.7) |
| Data scaling software | Aimless |
| Phasing software | PHASER (2.8.2) |
| Refinement software | BUSTER (2.11.7 (3-OCT-2019)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.000 | 1.868 |
| High resolution limit [Å] | 1.836 | 1.836 |
| Rmerge | 0.050 | 1.948 |
| Rmeas | 0.062 | 2.405 |
| Rpim | 0.036 | 1.392 |
| Number of reflections | 57259 | 2866 |
| <I/σ(I)> | 7.9 | 0.6 |
| Completeness [%] | 91.1 | 91.6 |
| Redundancy | 2.8 | 2.8 |
| CC(1/2) | 0.998 | 0.368 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.2 | 293 | 0.2M sodium chloride, 0.1M citrate-phosphate buffer pH 4.2, 20% PEG 8,000 |
