Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM30A |
| Synchrotron site | ESRF |
| Beamline | BM30A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-07-15 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9697 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 123.135, 61.309, 80.186 |
| Unit cell angles | 90.00, 117.42, 90.00 |
Refinement procedure
| Resolution | 54.650 - 2.630 |
| R-factor | 0.2225 |
| Rwork | 0.220 |
| R-free | 0.26900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.079 |
| Data reduction software | XDS |
| Data scaling software | pointless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 54.650 | 2.720 |
| High resolution limit [Å] | 2.630 | 2.630 |
| Number of reflections | 26769 | 2647 |
| <I/σ(I)> | 5.68 | |
| Completeness [%] | 94.8 | |
| Redundancy | 1.8 | |
| CC(1/2) | 0.985 | 0.586 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 288 | 2.8M sodium formate |
