Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM30A |
| Synchrotron site | ESRF |
| Beamline | BM30A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-07-15 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9697 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 122.922, 61.651, 80.111 |
| Unit cell angles | 90.00, 117.51, 90.00 |
Refinement procedure
| Resolution | 48.450 - 2.290 |
| R-factor | 0.21151 |
| Rwork | 0.208 |
| R-free | 0.27061 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.596 |
| Data reduction software | XDS |
| Data scaling software | pointless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.450 | 2.370 |
| High resolution limit [Å] | 2.290 | 2.290 |
| Number of reflections | 21606 | 1714 |
| <I/σ(I)> | 14.71 | |
| Completeness [%] | 88.1 | |
| Redundancy | 2 | |
| CC(1/2) | 0.910 | 0.797 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 2.8M sodium formate |
