8RUG
Crystal structure of Rhizobium etli L-asparaginase ReAV C189A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.046, 91.292, 105.697 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 69.090 - 1.700 |
R-factor | 0.1625 |
Rwork | 0.162 |
R-free | 0.18570 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.058 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.050 | 1.810 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.152 | 1.649 |
Rmeas | 0.158 | 1.721 |
Number of reflections | 83283 | 13254 |
<I/σ(I)> | 14.95 | 1.76 |
Completeness [%] | 99.9 | |
Redundancy | 13.2 | |
CC(1/2) | 0.999 | 0.665 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 292 | 20% PEG 8000, 0.2 M Li2SO4, 0.1 M Bicine pH 9.0 |