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8RU1

Chromatin remodeling regulator CECR2 with in crystallo disulfide bond

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I02
Synchrotron siteDiamond
BeamlineI02
Temperature [K]100
Detector technologyPIXEL
Collection date2014-11-30
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9794
Spacegroup nameC 1 2 1
Unit cell lengths87.910, 77.200, 78.140
Unit cell angles90.00, 91.22, 90.00
Refinement procedure
Resolution46.930 - 1.660
Rwork0.183
R-free0.21030
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.342
Data reduction softwarexia2
Data scaling softwarexia2
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0425)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.9301.700
High resolution limit [Å]1.6601.660
Number of reflections613334508
<I/σ(I)>18.2
Completeness [%]99.5
Redundancy3.4
CC(1/2)0.9990.768
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2933M sodium chloride 0.1M Bis-Tris pH 5.5

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