Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-08-21 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1.00 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 36.490, 56.900, 61.070 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.603 - 1.200 |
| Rwork | 0.161 |
| R-free | 0.17710 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.220 |
| Data reduction software | autoPROC |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 41.630 | 1.060 |
| High resolution limit [Å] | 1.000 | 1.000 |
| Rmeas | 0.057 | 1.114 |
| Number of reflections | 68875 | 10629 |
| <I/σ(I)> | 14.49 | 1.25 |
| Completeness [%] | 99.3 | 96.1 |
| Redundancy | 5.95 | |
| CC(1/2) | 0.999 | 0.532 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2.1 M DL-Malic acid pH 7.0 |
