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8RQW

Erk2 MAP kinase (T188E) AMP-PNP complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE MASSIF-1
Synchrotron siteESRF
BeamlineMASSIF-1
Temperature [K]100
Detector technologyPIXEL
Collection date2022-02-25
DetectorDECTRIS PILATUS3 2M
Wavelength(s)0.9655
Spacegroup nameP 1 21 1
Unit cell lengths48.913, 70.601, 60.409
Unit cell angles90.00, 109.61, 90.00
Refinement procedure
Resolution44.300 - 1.800
R-factor0.19777
Rwork0.196
R-free0.23058
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle1.643
Data reduction softwareMOSFLM
Data scaling softwareautoPROC
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0258)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.3001.830
High resolution limit [Å]1.8001.800
Number of reflections355282110
<I/σ(I)>7.80.9
Completeness [%]89.9
Redundancy3
CC(1/2)0.9790.587
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2930.1M sodium hepes pH=7, 4% v/v PEG 400 and 2M ammonium sulfate.

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PDB entries from 2025-07-09

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