Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-07-26 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.95374 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 69.748, 69.748, 72.827 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 60.400 - 1.791 |
| R-factor | 0.2225 |
| Rwork | 0.220 |
| R-free | 0.26170 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.990 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8 (24-FEB-2021)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.404 | 2.003 |
| High resolution limit [Å] | 1.791 | 1.791 |
| Number of reflections | 12352 | 620 |
| <I/σ(I)> | 12.8 | |
| Completeness [%] | 83.1 | |
| Redundancy | 13 | |
| CC(1/2) | 0.998 | 0.643 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | sodium citrate 0.3M, PCTP pH 6 |
