8ROG
Human cohesin SMC1A-HD(shortCC-EQ)/RAD21-C complex - ATPgS-Mg-bound conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-05-05 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.000008 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 66.219, 113.984, 134.071 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.540 - 1.940 |
R-factor | 0.2071 |
Rwork | 0.204 |
R-free | 0.25330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.881 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17_3644) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.060 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.166 | 2.389 |
Number of reflections | 37968 | 5996 |
<I/σ(I)> | 10.95 | 1.06 |
Completeness [%] | 99.8 | 99 |
Redundancy | 12.9 | 11.7 |
CC(1/2) | 0.999 | 0.366 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M sodium formate; 0.1 M Bis Tris propane pH 6.5; 20 % w/v PEG 3350 |