8RNT

STRUCTURE OF RIBONUCLEASE T1 COMPLEXED WITH ZINC(II) AT 1.8 ANGSTROMS RESOLUTION: A ZN2+.6H2O.CARBOXYLATE CLATHRATE

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	48.710, 46.510, 41.140
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.14
RMSD bond length	0.024
RMSD bond angle	0.057
Refinement software	PROFFT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.800 *	1.800 *
Total number of observations	9459 *
Number of reflections	8291 *
Completeness [%]		91 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	reservior	MPD	55 (%(v/v))
3	1	reservoir	sodium acetate	20 (mM)
4	1	reservoir	zinc acetate	2 (mM)