Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-03-24 |
| Detector | DECTRIS EIGER X 4M |
| Wavelength(s) | 0.9998 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 34.490, 57.740, 61.530 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.702 - 1.200 |
| Rwork | 0.162 |
| R-free | 0.18630 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.262 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.765 | 1.220 |
| High resolution limit [Å] | 1.150 | 1.150 |
| Rmeas | 0.073 | 1.010 |
| Number of reflections | 83428 | 13324 |
| <I/σ(I)> | 7.26 | 0.7 |
| Completeness [%] | 98.9 | |
| Redundancy | 3.15 | 2.55 |
| CC(1/2) | 0.998 | 0.457 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 2.4 M Sodium malonate pH 7.0 (Index/C3) |
