8R9T
Crystal structure of the C-terminal domain of Chlamydomonas reinhardtii CFAP410
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-11-06 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97242 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.435, 48.097, 53.156 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.790 - 1.400 |
R-factor | 0.1649 |
Rwork | 0.163 |
R-free | 0.18860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 0.922 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.18_3845) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.136 | 1.019 |
Rmeas | 0.142 | 1.074 |
Rpim | 0.040 | 0.331 |
Number of reflections | 22256 | 19011 |
<I/σ(I)> | 9.4 | 1.11 |
Completeness [%] | 98.2 | 87.57 |
Redundancy | 12.5 | 9.9 |
CC(1/2) | 0.995 | 0.750 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 0.02 M CaCl2, 0.1 M sodium acetate (pH 5.0), 30% (v/v) 2-Methyl-2,4-pentanediol |