8R5D
Crystal structure of human TRIM7 PRYSPRY domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-10-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000030 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.258, 70.905, 85.503 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.790 - 1.800 |
R-factor | 0.20589 |
Rwork | 0.204 |
R-free | 0.23940 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.496 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.350 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.113 | 0.898 |
Rmeas | 0.122 | 0.973 |
Rpim | 0.047 | 0.371 |
Total number of observations | 237490 | 13884 |
Number of reflections | 35213 | 2068 |
<I/σ(I)> | 7.2 | 2 |
Completeness [%] | 99.9 | |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 0.996 | 0.884 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.2 M Sodium malonate dibasic monohydrate pH 7.0, 20 % PEG3350 |