8R5B
Crystal structure of human TRIM7 PRYSPRY domain bound to (3-phenoxybenzoyl)-L-glutamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-09-09 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000000 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 41.189, 87.436, 122.242 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.760 - 1.600 |
R-factor | 0.15028 |
Rwork | 0.148 |
R-free | 0.18684 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.634 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.760 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.075 | 0.255 |
Rmeas | 0.082 | 0.276 |
Rpim | 0.031 | 0.106 |
Total number of observations | 19038 | |
Number of reflections | 59265 | 2879 |
<I/σ(I)> | 13.8 | 6.1 |
Completeness [%] | 100.0 | |
Redundancy | 6.8 | 6.6 |
CC(1/2) | 0.997 | 0.964 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 2M NaCl 100 mM acetate pH 4.5 |