8QZR
SARS-CoV-2 delta RBD complexed with BA.4/5-9 Fab
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-07-01 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.97624 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 251.576, 251.576, 251.576 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 59.300 - 3.770 |
| R-factor | 0.2531 |
| Rwork | 0.251 |
| R-free | 0.29970 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.524 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.000 | 3.840 |
| High resolution limit [Å] | 3.770 | 3.770 |
| Rmerge | 0.414 | |
| Rpim | 0.065 | |
| Number of reflections | 26729 | 1322 |
| <I/σ(I)> | 8 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 41.8 | |
| CC(1/2) | 0.998 | 0.351 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M BIS-TRIS pH 6.5, 2% v/v Polyethylene glycol monomethyl ether 550, 1.8 M Ammonium sulfate |
