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8QVV

Crystal structure of Ompk36 GD at 3500 eV based on analytical absorption corrections

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I23
Synchrotron siteDiamond
BeamlineI23
Temperature [K]80
Detector technologyPIXEL
Collection date2021-05-20
DetectorDECTRIS PILATUS 12M
Wavelength(s)3.54
Spacegroup nameC 1 2 1
Unit cell lengths232.078, 74.700, 91.350
Unit cell angles90.00, 112.21, 90.00
Refinement procedure
Resolution107.430 - 2.340
R-factor0.19473
Rwork0.193
R-free0.23277
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.450
Data reduction softwareDIALS
Data scaling softwareDIALS
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0415)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]107.4302.424
High resolution limit [Å]2.3402.340
Number of reflections606595633
<I/σ(I)>21.37
Completeness [%]98.8
Redundancy11
CC(1/2)0.9970.874
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.62930.1M Lithium sulfate, 0.1M sodium citrate pH 5.6 and 12% PEG4000

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