8QV9
Hexameric HIV-1 CA in complex with DDD01829021
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9159 |
Spacegroup name | P 6 |
Unit cell lengths | 90.327, 90.327, 56.509 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.230 - 1.760 |
R-factor | 0.20258 |
Rwork | 0.200 |
R-free | 0.24552 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.022 |
RMSD bond angle | 2.035 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.280 | 1.810 |
High resolution limit [Å] | 1.760 | 1.760 |
Rmerge | 0.100 | 0.810 |
Number of reflections | 26170 | 1924 |
<I/σ(I)> | 11.6 | 2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.9 | 9 |
CC(1/2) | 0.990 | 0.460 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 290 | 0.1M Tris buffer, pH 8.0 to 9.0, 10-15% PEG550MME, 0.15M KSCN |