8QQF
TBC1D23 PH domain complexed with STX16 TLY motif
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-05 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.997 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 134.159, 134.159, 123.542 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 67.080 - 2.190 |
R-factor | 0.2163 |
Rwork | 0.214 |
R-free | 0.25650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 0.971 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (dev_svn+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 200.000 | 2.480 |
High resolution limit [Å] | 2.190 | 2.190 |
Rmerge | 0.133 | |
Number of reflections | 14895 | 745 |
<I/σ(I)> | 23 | |
Completeness [%] | 94.8 | 100 |
Redundancy | 32.7 | 82.9 |
CC(1/2) | 0.700 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289.15 | 0.8M Potassium phosphate dibasic, 0.1M HEPES/NaOH pH 7.5, 0.8M Sodium phosphate monobasic and 1% 1,2-Butandiol |