8QQC

Crystal structure of Lymantria dispar CPV14 polyhedra single crystal

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE VMXm
Synchrotron site	Diamond
Beamline	VMXm
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-09-29
Detector	DECTRIS EIGER2 X CdTe 9M
Wavelength(s)	0.5814
Spacegroup name	I 2 3
Unit cell lengths	103.102, 103.102, 103.102
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.450 - 1.300
R-factor	0.2304
Rwork	0.229
R-free	0.25660
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.882
Data reduction software	DIALS
Data scaling software	xia2.multiplex
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.100	1.320
High resolution limit [Å]	1.300	1.300
Rmerge	0.304	0.910
Rpim	0.146	0.696
Number of reflections	40615	1275
<I/σ(I)>	3.7	0.5
Completeness [%]	90.7	57.69
Redundancy	4.5	2.02
CC(1/2)	0.911	0.356

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	IN CELL	7.5	300	In vivo