8QN9
OPR3 variant - R283E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-03-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 87.680, 89.780, 49.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.840 - 1.600 |
R-factor | 0.1539 |
Rwork | 0.152 |
R-free | 0.18180 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.154 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_4761: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.840 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 48262 | 1770 |
<I/σ(I)> | 15.41 | |
Completeness [%] | 92.4 | |
Redundancy | 6.5 | |
CC(1/2) | 0.998 | 0.458 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 100 mM MES/Tris, 50 mM ammonium sufate, 14% PEG8000 |