8QKY
Bacteriophage T5 dUTPase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 43 |
Unit cell lengths | 78.430, 78.430, 86.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.760 - 2.000 |
R-factor | 0.1793 |
Rwork | 0.178 |
R-free | 0.21090 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.843 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.070 | 1.010 |
Number of reflections | 35488 | 2637 |
<I/σ(I)> | 22.91 | 1.86 |
Completeness [%] | 99.9 | |
Redundancy | 12.76 | |
CC(1/2) | 0.990 | 0.710 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 296 | 0.075 M TRIS hydrochloride, 1.5 M Ammonium sulfate, 25% v/v glycerol |